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ANALYTICAL CHEMISTRY I

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Learning Outcomes

  • Will explain the nature of analytical chemistry.
  • Explains the importance of analytical chemistry.
  • Explains the classification of quantitative analytical methods.
  • Explains the typical steps of a quantitative analysis process in order.
  • Will explain the selection and use of reagents and other chemicals.
  • Explains the classification of chemical substances according to their purity.
  • Explains the usage rules for reagents and solutions.
  • Will provide information on the cleaning and labeling (marking) of laboratory materials.
  • Explains the cleaning rules for laboratory materials.
  • Lists the auxiliary tools used in the laboratory and explains their purposes.
  • Explains the labeling rules for laboratory materials.
  • Will explain general procedures related to weighing.
  • Explains the types of analytical balances.
  • Explains the use of analytical balances.
  • Explains the precautions in using analytical balances.
  • Explains the sources of errors in weighing.
  • Explains the materials used in weighing and their purposes.
  • Explains the weighing methods according to the properties of the substances.
  • Will explain basic operations performed in the laboratory.
  • Explains the precipitation process and the tools used.
  • Explains the materials used in filtration and their purposes.
  • Explains the sequential process of filtration and incineration of precipitates.
  • Explains the rules for handling heated objects.
  • Will explain the measurement of volume.
  • Lists the units of volume.
  • Explains the effect of temperature on volume measurements.
  • Explains the instruments and their purposes for precise volume measurements.
  • Explains the use of volumetric containers.
  • Will explain the calibration of volumetric containers.
  • Explains the containers that require volumetric adjustment.
  • Explains the rules of calibration.
  • Will explain percent-based and density-based solutions.
  • Solves problems involving weight/weight concentration.
  • Solves problems involving weight/volume concentration.
  • Solves problems involving volume/volume concentration.
  • Solves problems involving percentage and density-based solutions.
  • Will explain normality.
  • Explains and calculates normality.
  • Explains and calculates the equivalent factor.
  • Explains and calculates the equivalent weight.
  • Solves problems where solution concentrations are given in normality.
  • Converts concentrations given in normality to other concentration expressions.
  • Will explain molarity.
  • Explains and calculates molarity.
  • Solves problems where solution concentrations are given in molarity.
  • Converts concentrations given in molarity to other concentration expressions.
  • Will explain molality, formality, and osmolarity.
  • Explains and calculates molality, formal concentration, and osmolarity.
  • Solves problems where solution concentrations are given in molality or osmolarity.
  • Converts concentrations given in molality or osmolarity to other concentration expressions.
  • Will explain how valence numbers are determined.
  • Distinguishes between oxidized and reduced species.
  • Explains the basic rules for finding the valence.
  • Calculates the valence numbers of atoms in molecules.
  • Will explain reaction balancing.
  • Explains the fundamental laws on which chemical reactions are based.
  • Balances ion-exchange reactions.
  • Balances electron-exchange reactions.
  • Will explain basic stoichiometric calculations.
  • Calculates the stoichiometric factor.
  • Converts mass to mols and mols to mass according to the reaction equation.
  • Calculates the mol numbers of reactants, products, and remaining components according to the reaction equation.
  • Calculates the mass of reactants, products, and remaining components according to the reaction equation.
  • Will explain complex stoichiometric calculations.
  • Calculates the quantities of substances in stoichiometry problems that require multi-step concentration calculations.
  • Performs calculations in stoichiometry problems based on reaction types.
  • Performs calculations in back titration applications.
  • Will explain chemical equilibrium and equilibrium constant.
  • Classifies electrolytes.
  • Defines acids and bases.
  • Matches conjugate acids and bases.
  • Explains the state of chemical equilibrium.
  • Explains Le Chatelier's principle.
  • Will explain types of chemical equilibrium.
  • Distinguishes between different types of equilibrium constants.
  • Establishes the equilibrium constants of reactions.
  • Will explain the ionization of water.
  • Calculates the concentrations of hydronium and hydroxide ions in water ionization.
  • Will explain the ionization of acids and bases.
  • Explains the ionization of acids and bases.
  • Establishes the ionization constants of weak acids/bases.
  • Calculates the ionization constant of weak acids/bases using the ionization constant of water.
  • Calculates the hydronium ion concentration in weak acid solutions.
  • Calculates the hydroxide ion concentration in weak base solutions.
  • Will explain buffer solutions.
  • Lists the properties of buffer solutions.
  • Distinguishes between equilibria in buffer solutions.
  • Calculates the hydronium ion concentration and pH in buffer solutions.
  • Solves problems involving the addition of a strong base to buffer solutions.
  • Solves problems involving the addition of a strong acid to buffer solutions.
  • Calculates the buffer capacity of buffer solutions.
  • Will explain ionic strength.
  • Explains ionic strength.
  • Calculates the ionic strength of solutions.
  • Will explain activity.
  • Explains the activity of species.
  • Explains the activity coefficients of species.
  • Explains the Debye-Hückel equation.
  • Will explain dissolution equilibria.
  • Explains the dissolution of solids in water.
  • Explains the dissolution of gases in water.
  • Explains and calculates the solubility product constant.
  • Will explain the common ion effect.
  • Explains the common ion.
  • Explains and calculates the effect of the common ion on equilibria.
  • Will explain the effect of foreign ions.
  • Uses the concept of activity.
  • Uses activity coefficients.
  • Uses the Debye-Hückel Equation and its derivatives.
  • Calculates the effect of activity on solubility equilibria.
  • Will explain solubility constants.
  • Uses the dissolution constant.
  • Explains the concept of a saturated solution.
  • Calculates the concentration of a sparingly soluble salt in water.
  • Will explain multiple dissolution equilibria.
  • Calculates the concentrations in situations with multiple dissolution equilibria.
  • Calculates the precipitation sequence in cases of multiple dissolution equilibria.
  • Calculates selective precipitation.
  • Will explain gravimetry.
  • Explains the concept of mass.
  • Explains gravimetric methods.
  • Explains the conservation of mass.
  • Will explain precipitation gravimetry.
  • Explains the theory and applications of precipitation gravimetry.
  • Explains the quantitative applications of precipitation gravimetry.
  • Explains the qualitative applications of precipitation gravimetry.
  • Calculates the results of precipitation gravimetry.
  • Will explain volatilization gravimetry.
  • Explains the theory and applications of volatilization gravimetry.
  • Explains thermogravimetry.
  • Explains the quantitative applications of volatilization gravimetry.
  • Calculates the results of volatilization gravimetry.
  • Will explain method selection.
  • Lists the important factors in method selection.
  • Selects the method based on the properties of the analyte and the environment.
  • Lists the factors to be considered in method development.
  • Will explain sample preparation.
  • Explains the factors to be considered in sampling.
  • Explains how to prepare the sample according to the analyte.
  • Explains how to prepare the sample according to the method.
  • Explains how to prepare the sample according to the environment.
  • Will explain sources of error in chemical analysis.
  • Uses significant figures in expressing analysis results.
  • Explains and exemplifies the sources of errors in chemical analysis.
  • Explains the types of errors in chemical analysis.
  • Will explain the evaluation of analytical data.
  • Defines and calculates the confidence interval.
  • Performs hypothesis testing to evaluate analysis results.
  • Calculates the T-test, F-test, and Q-test in analysis results.
  • Compares two analytical data sets in various aspects.
  • Will explain method validation.
  • Defines method validity.
  • Explains the importance and necessity of method validity.
  • Lists the parameters of method validity.
  • Classifies the parameters of method validity according to official sources.
  • Will explain parameters of analytical method validation.
  • Defines selectivity and explains how it is determined.
  • Defines stability and explains how it is determined.
  • Defines linearity and explains how it is determined.
  • Defines the detection limit and explains how it is determined.
  • Defines the limit of quantification and explains how it is determined.
  • Defines precision and explains how it is determined.
  • Defines accuracy and explains how it is determined.
  • Defines robustness and explains how it is determined.
  • Will explain the laboratory environment and basic rules.
  • Explains the basic rules to be followed in the laboratory
  • Lists the laboratory materials to be brought to the laboratory.
  • Lists the materials to be brought for protection to the laboratory and explains their usage.
  • Will identify the laboratory bench and equipment.
  • Explains the bench layout.
  • Distinguishes between deionized water and tap water, and explains their usage.
  • Distinguishes between waste containers and explains their usage.
  • Will explain qualitative analysis.
  • Defines qualitative analysis.
  • Explains the goal of qualitative ion analysis.
  • Will explain basic laboratory procedures.
  • Distinguishes the main chemical properties of reagents.
  • Explains how to add reagents to the reaction environment.
  • Distinguishes decantation and explains its usage.
  • Distinguishes complete precipitation and explains its usage.
  • Distinguishes litmus paper and explains its usage.
  • Distinguishes deionized water and explains its usage.
  • Explains how to clean the materials.
  • Lists the reagents used in the analysis of the first group anions.
  • Will explain the analysis of anions.
  • Lists the first group anions.
  • Lists the reasons for using reagents in the analysis of the first group anions.
  • Will explain the analysis of chloride ion.
  • Lists the reactions of chloride ions.
  • Explains the identification reaction of chloride ions.
  • Writes the equation of the identification reaction of chloride ions.
  • Will explain the analysis of sulfate ion.
  • Lists the reactions of sulfate ions.
  • Explains the identification reaction of sulfate ions.
  • Writes the equation of the identification reaction of sulfate ions.
  • Will explain the analysis of nitrate ion.
  • Lists the reactions of nitrate ions.
  • Explains the identification reaction of nitrate ions.
  • Writes the equation of the identification reaction of nitrate ions.
  • Will explain the analysis of phosphate ion.
  • Lists the reactions of phosphate ions.
  • Explains the identification reaction of phosphate ions.
  • Writes the equation of the identification reaction of phosphate ions.
  • Will explain the analysis of carbonate ion.
  • Lists the reactions of carbonate ions.
  • Explains the identification reaction of carbonate ions.
  • Writes the equation of the identification reaction of carbonate ions.
  • Will explain the analysis of an unknown sample containing anions.
  • Defines the identification reactions of the first group anions.
  • Distinguishes the analysis environments of the first group anions.
  • Distinguishes the products and their properties formed as a result of the identification reactions of the first group anions.
  • Determines the sample content based on the properties of the products formed in the experiment.
  • Will explain the basic procedures in solution preparation.
  • Performs stoichiometric calculations.
  • Prepares a solution of known concentration and volume from a liquid standard substance.
  • Prepares a solution of known concentration and volume from a solid standard substance.
  • Will explain the analysis of Group I cations.
  • Lists the group I cations.
  • Distinguishes the common precipitating reagent of the group I cations.
  • Will explain the systematic analysis of Group I cations.
  • Explains the systematic analysis of the group I cations.
  • Writes the reaction equations of the group I cations.
  • Distinguishes the compounds and colors formed as a result of the identification reactions of the group I cations.
  • Distinguishes the analysis environments of the group I cations.
  • Will explain the Group III-A cations.
  • Lists the group III-A cations.
  • Distinguishes the common precipitating reagent of the III-A group cations.
  • Will explain the systematic analysis of Group III-A cations.
  • Explains the systematic analysis of the III-A group cations.
  • Writes the reaction equations of the III-A group cations.
  • Distinguishes the compounds and colors formed as a result of the identification reactions of the III-A group cations.
  • Distinguishes the analysis environments of the III-A group cations.
  • Will explain the analysis of Group V cations.
  • Lists the group V cations.
  • Lists the reagents used in the analysis of the group V cations.
  • Lists the reasons for using reagents in the analysis of the group V cations.
  • Will explain the analysis of sodium ion.
  • Lists the reactions of sodium ions.
  • Will explain the analysis of potassium ion.
  • Lists the reactions of potassium ions.
  • Explains the identification reaction of potassium ions.
  • Writes the equation of the identification reaction of potassium ions.
  • Will explain the analysis of ammonium ion.
  • Lists the reactions of ammonium ions.
  • Explains the concept of a witness experiment.
  • Explains the identification reaction of ammonium ions.
  • Writes the equation of the identification reaction of ammonium ions.
  • Will explain the analysis of magnesium ion.
  • Lists the reactions of magnesium ions.
  • Explains the identification reaction of magnesium ions.
  • Writes the equation of the identification reaction of magnesium ions.
  • Will explain the systematic analysis of Group I-V cations.
  • Explains the principles of the systematic analysis of I-V group cations.
  • Systematically distinguishes I-V group cations.
  • Will explain quantitative analysis.
  • Defines quantitative analysis.
  • Explains the goal of quantitative analysis.
  • Will explain the precipitation process.
  • Explains the precipitation setup.
  • Distinguishes the importance of complete precipitation in gravimetry.
  • Defines the formed reaction and precipitate.
  • Will explain the filtration process.
  • Explains the filtration setup.
  • Distinguishes the filter papers to be used.
  • Explains the ashless filter paper.
  • Lists and distinguishes the folding types of filter paper.
  • Will explain the combustion process.
  • Lists the laboratory materials they will use.
  • Explains the muffle furnace.
  • Explains the temperature and duration of the combustion process.
  • Explains the temperature and duration of the combustion process.
  • Explains the desiccator.
  • Will explain the weighing process.
  • Explains the weighing conditions.
  • Explains the process of reaching full tare.
  • Will explain analytical calculations.
  • Explains the gravimetric factor.
  • Calculates the sulfate amount from the formed barium sulphate precipitate.
  • Will explain statistical calculations for repeated measurements.
  • Lists the statistical concepts used for repeated measurements.
  • Calculates the mean using experimental results.
  • Calculates the standard deviation using experimental results.
  • Calculates the variance using experimental results.
  • Applies calculations related to confidence intervals to experimental data.
  • Presents the statistically calculated quantitative results with error.
  • Will explain significance tests.
  • Applies hypothesis testing to evaluate the analysis results.
  • Applies T-test, F-test, and Q-test to the analysis results.
  • Compares two analytical data sets obtained from experimental results in various aspects.
  • Interprets the data obtained from significance tests.
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